Container nozzle construction



Nov. 29, 1955 E. A. SANFORD CONTAINER NOZZLE CONSTRUCTION 3 Sheets-Sheet 1 Filed March 24, 1951 M R v INVENTOR. ELBERT A. SANFORD ms ATTORNEY Nov. 29, 1955 E. A. SANFORD 2,725,159

CONTAINER NOZZLE CONSTRUCTION Filed March 24, 1951 3 Sheets-Sheet 2 IN V EN TOR.

ELBERT A. SANFORD BY HIS A TTORNEY Nov. 29, 1955 E. A. SANFORD 2,725,159

CONTAINER NOZZLE CONSTRUCTION Filed March 24, 1951 3 Sheets-Sheet 3 IN VEN TOR. ELBERT A. SANFORD HIS 4T 7' OR/VE Y United States Patent 2,725,159 CONTAINER NOZZLE CONSTRUCTION Elbert A. Sanford, Irondequoit, N. Y., assignor to The Pfaudler C0,, Rochester, N. Y., a corporation of New York Application March 24, 1951, Serial No. 217,345 6 Claims. (Cl. 220-64) This invention relates to container nozzle constructions and, more particularly, to the variety thereof adapted for use in combination with containers for processing corrosive materials such as acid or alkaline substances. To afford the necessary strength, such containers have been commonly made of iron or steel with Walls of substantial thickness or rigidity. Such containers usually have a plurality of integrally formed nozzles oropenings through which the materials are passed, orthrough which agitators, sampling tubes, thermometers and the like may be inserted. To protect the container and nozzle against corrosion, it has been a common practice to provide their inner walls with a glass or enamel coating. In the use of this equipment, it has been found that mechanical strains may be set up in pipe lines connected to these nozzles, and these strains may be transmitted to the containers, causing the glass coating to crack or craze, especially over curved sections. Such strains may be caused by physical movement in the pipe line, as in making or breaking a flanged connection, or operating a valve. Again, they may result from expansion and contraction of the pipe, resulting from temperature changes. Another cause of corrosion of nozzle openings is the use of unsuitable porous gaskets to protect glass coated flange surfaces, which permit corrosive liquids to seep through gasketed joints and come into contact with the uncoated outer portions of the nozzle flange, so that the glass coating may be undermined. As many of these containers or tanks are of large size, the difliculties involved in dismantling and returning them to the factory for repairs is well understood and appreciated in the art.

One object of the invention, therefore, is to provide an improved corrosion-resistant container nozzle construction of a more effective and practical character.

Another object is to provide a construction of the above nature adapted for making satisfactory repairs in the field.

Another Object is to provide a construction having the above advantages and which is readily adaptable to protect various sections of said nozzle.

A further object is to provide a container nozzle construction having the above advantages and comprising parts adapted to be readily and economically manufactured and assembled.

To these and other ends the invention resides in certain improvements and combinations of parts, all as will be hereinafter more fully described, the novel features being pointed out in the claims at the end of the specification.

In the drawings:

Fig. 1 is an enlarged sectional elevation of a portion of a container or tank having a nozzle located eccentrically on its upper pressure head and showing in detail the application of a nozzle. shield to the inner swaged throat portion of said nozzle and container;

Fig. 2 shows similar container and nozzle portions but having the shield applied over the outer throat and flange of said nozzle;

Fig. 3 is similar to Fig. 2 but shows a somewhat modified construction;

2,725,159 Patented Nov. 29, 1955 Fig. 4 is a view of a similar container nozzle but shows a two-part shield covering the entire nozzle and flange;

Fig. 5 shows a similar container nozzle with a threepart shield covering the nozzle and flange;

Fig. 6 is an enlarged sectional elevation of a portion of a container having a nozzle located concentrically in its bottom head and showing a shield covering the inner throat of said nozzle and the adjoining swaged. portion of the container;

Fig. 7 is a view similar to Fig. 6 but showing the shield applied to the outer throat portion of the nozzle and its flange, and

Fig. 8 is a view similar to Fig. 7 but showing a twopart shield covering the entire nozzle throat and its flange and showing the connection therewith of a communicating pipe line.

The preferred embodiment of the invention, herein disclosed by way of illustration, comprises a processing container or tank of the known variety, for example, having cylindrical side walls of heavy sheet metal, such as mild steel plate, with dished or domed upper and lower pressure heads 15 and 16, respectively. Such tanks are commonly providedwith nozzles connected to the heads or side walls thereof, for the supply or delivery of materials, or for access to the interior for other purposes, as for inserting dip pipes, thermometer wells, or the like. In the present instance, by way or" illustration, the nozzles are shown as communicating through the tank heads, either eccentrically, as shown generally at 17, Figs. 1 to 5, inclusive, or concentrically, as shown at 18, Figs. 6to 8, inclusive. These nozzles are usually formed by swaging outwardly a portion 19 of the container head or Wall to form a nozzle and welding thereto a short section 20 of pipe formed with a flange 21, as shown in the drawings and as well understood in the art. This connects the flanged nozzle with the head or wall of the container by a smoothly curved, swaged shoulder portion 22.

The inner surfaces of such a tank employed in processing corrosive substances are commonly coated and protected by a fused ceramic coating 23, of glass or enamel of suitable composition, as wellunderstood in the art, extending continuously over the inner wall and nozzle surfaces and over the outer surface of the nozzle flange, as shown.

I have found that any one or more of those exposed, curved or otherwise uneven nozzle portions, where the glass coating is most likely to become damaged, can be effectively repaired, in the installed location of the tank, by the application thereto of one or more protective shield sections made of flexible, thin, corrosion-resisting metal, such as tantalum or the like, known to be resistant to corrosion by acid or alkaline materials to be handled.

Thus, to repair and protect the swaged and curvedportion 22 adjacent the inner end of the nozzle, I apply a sheet or plate 24 (Fig. l) of thin, corrosion-resisting metal, such as tantalum, having a thickness, for example, of 0.03 of an inch and readily shaped to lit the coated and curved surface of the container about the swaged shoulder of the nozzle. This plate is formed with a central opening around which it is spun outwardly, as at 25, to substantially fit the inner swaged portion of the nozzle, preferably in asomewhat spaced relation, as shown. The space between this shield portion and the coated surfaces of the tank and nozzle are preferably filled with a layer 26 of corrosion-resisting resin or silicate cement, such as the commercially available Alkor or Penchlor cements, depending upon the chemical conditions to be met. The inner plate portion 24 of the shield is further secured to the wall of the container by a ring of circumferentially spaced stud bolts 27 made of tantalum or other known corrosion-resisting metal, the

bolts bein'g screwed into holes tapped part way through the tank wall, as shown. To insure a more perfect seal, the edge of the plate portion 24 is mounted on a gasket 28 of corrosion-resisting material, such, for example, as the commercially known Teflon or the like, having a thickness of 0.05 of an inch. The nuts 29 of the stud bolts serve to draw the periphery of the plate and" the gasket against the interposed layer of cement, the margin 3,0 of the plate being preferably formedwith a nar; row flange turned inwardly to retain and protect the cement, thus forming a tight seal between the plate and the coated surface of the container. The outer end 3-1 of the sleeve portion of the shield' is also formed with a narrow flange turned outwardly for contact with the coated surface of the nozzle to similarly protect and retain the interposed cement and form a substantially smooth and tight joint between the sleeve andthe-nozzle throat.

It is apparent that by this construction, the plate portion 24 and its sleeve portion 25 are effectively secured and sealed to the glass coated surfaces which theycover, so as to prevent the access thereto of the corrosive materials in the tank, thus protecting such parts against pitting at portions of the glass coating which may have become cracked or crazed in use.

It is often desirable to protect the outer end of the nozzle throat and the outer surface of its flange when the ceramic coating of such parts has been damaged. In such cases, a plate 32 of tantalum, Fig. 2, having a thickness, for example, of 0.03 of an inch, is cut to fit and completely cover the flange 21 andformed with a central opening around which the plate is spun inwardly to form an inwardly extending sleeve 33' fitting the coated outer end of the throat of the nozzle in slightly spaced relation. The space between the sleeve and nozzle is filled with a layer of corrosion-resisting cement 34, as described above and the inner end of the sleeve portion is preferably turned or flanged outwardly as at- 35 to engage the coated surface of the nozzle, thus protecting and retaining the cement and forming a substantially smooth and continuous joint with the throat.

In forming such outer shield'portions, by spinning them from a plate, as described, it has been found that-there is a practical limit to the extent to which suitable metals may be spun to form the inwardly extending nozzle; sleeve and it has been found desirable in some applications, as in eccentrically positioned nozzles-of tank heads, to form such nozzle portions by using a tube section ofthe desired diameter to form the nozzle sleeve and pressing oneend of the tube outwardly to form a flange portion to partially cover the nozzle flange. Thus, as shownin Fig. 3, a section of tubing 36 is employed; to form a nozzle sleeve of suitable diameter for lying within the nozzle throat in slightly spaced relation as shown. The outer end of the sleeve is pressed outwardly to form a flange 37 which, from practical considerations, is of limited width and only partially covers the coated outer surface of the nozzle flange 21. A ring 38 of tantalumis shaped tofitaround and lie under the outwardly fla'ngedend 37 of the tube and to cover the coated outer surface of the nozzle flange 21. A layer 39 of-corrosion-resisting cement is interposed between the shield and ring parts and the nozzle, as shown, to secure the shield in place and'seal itsjoint with the nozzle and the inner end'of the sleeve portion is turned or flanged outwardly asat 40 'to protect and retain the cement. This modified construction completely covers and protects the outer throat and flange surface, as described above, and has the additionaladvantage thatthe tube 36 may be extended asfar as desired into the nozzle-so as to cover the welded join't 41-between the nozzle 19 and its flange member '20-at'an y, distance at which this welded joint may lie from the nozzle flange.

The invention is adaptable also to cases in' whichboth the swaged inner end of the nozzle and its outwardly flanged portion may have become damaged. In such 'erally ofshorter length and symmetrical shape.

situations, use may be made of both of the shield portions described above andshown in- Figs. 1- and 2, with an interposed connecting sleeve or Dutchman. Thus, as shown in Fig. 5, the swaged inner end of the throat may be protected by a plate 42 having an outwardly spun sleeve 43 substantially fitting the nozzle throat, this shield portion being secured, as, before to the container by stud bolts 44, and further secured and sealed by corrosion-resisting cement 45. The outer shield portion 46 is constructed and, applied as. described above in connection with the constructionshown in Fig. 2, except that the inner end of its sleeve portion 47 and the inner end of sleeve portion 43. of the inner plate 42 are left straight and unflanged', as shown. A section of tubing 48, or Dutchman, has its; inner end 49 fitted into the outer end of sleeve 43 and its outer end 50 fitted over the inner end of sleeve 47, so as to provide a continuous shield over the entire nozzle including its swaged. inner shoulder and'its outer flange surface, The layer of securing and sealing content is continued throughout the space between the three; shield portions and the portions of the nozzle so as to also seal' the joints between the shield portions and provide altogether a complete protection for the coated nozzle surface; Since the sleeve portion 48, is formed from a tube, it, may be made of any suitable length for a nozzle of any length.

A similar-complete shield may be made in two parts by employing the modified construction of the outer shield portion shown in Fig. 3'. Thus, as shown in Fig. 4, an inner shield portion 51 is formed and secured as described above in connection with Fig. 5. In this case, however, the outer shieldportion is formed from a section of tubing 52' having itsinner end 53 fitted within the end of sleeve portion ofplate 51, while its other end is pressed outwardly'to-form a flange 54 partly covering the outer surface of the, nozzle flange 21-. A ring 55 is cut to fit about and lie under flange 54 and completely cover the outer surface of the nozzle flange, as shown. A continuous layer 56 of cement is interposed between the-shield portions and nozzle'for'the purposes described. In-this construction, since the sleeve'portion 52 is formed from tubing, it may be made of any desired length to suit the length of the nozzle.

Figs. 6, 7 and 8 show adaptations of the invention to nozzles located concentrically in the dished bottom head orin the side walls of a container, such nozzles being gen- Fig. 6 shows an inner shield portion generally similar to that described above in connection. with Fig. 1, formed from a plate 57 secured to the-contai-ner wall by a plurality of stud bolts 58, withaninterposed gasket 5? and a layer of cement 60, as described above. In this case, the sleeve portion 61-; spun outwardly from the plate, may usually be extended tocover the welded connection 62 between the shorter swaged nozzle 63' of the container and the flanged nozzle member 64'. The outerend 65 of the sleeve portion is preferablyflanged orturned-outwardly as at 66 to retain and protect the cement and maintain a substantially smooth and continuous joint with thenozzle throat, as previously described.

Fig. 7 shows the adaptation to a shorter symmetrical nozzle, such as referred to, ofan outer shield portion similar to thatdescribed'inconnection'with Fig. 2, a-plate 67 being formed to completely cover the outer coated surface of the nozzle-flange and spun to form a nozzle sleeve 68. In this case also the sleeve may usually be spun in sufiicient length to-cover the-welded connection 62 between the-swaged nozzle portion 63' and its flanged outer member 64'. This shield-portion is secured and sealed as before by interposed layer 69- of corrosionresisting cement.

In the event that a nozzle has become-damaged at both its inner swaged portion and-its outer flangeportion, the invention may be employed to provide complete protection for both such portions. For this purpose,

as shown in Fig. 8, use may be made of an inner shield portion 70 generally similar in construction and arrangement to those described above in connection with Figs. 4 and 5. The outer end of its sleeve portion 71 is fitted closely within the inner end 72 of the sleeve of an outer shield portion 73, spun from the plate substantially as described above in connection with Fig. 5, the joint between the shield portions and the spaces between them and the nozzle being sealed by a securing layer of cement 74, as shown. This figure shows such a shielded nozzle connected to a communicating pipe line 75 with an interposed gasket 76. The flange 77 of the pipe line is secured to the flange member 64 of the nozzle by bolts 78 and nuts 79, as well understood in the art.

This application is a continuation in part of my copending application Serial No. 134,513, filed December 22, 1949, for Container Nozzle Construction, and now abandoned. Certain parts of the subject matter herein disclosed but not claimed are disclosed and claimed in my divisional application, Serial No. 302,153, filed August 1, 1952, now Patent No. 2,714,470.

It is apparent from the above description that the invention provides means for effectively covering and protecting any portion of a tank nozzle which may have its ceramic lining damaged, so as to prevent corrosive attack of the underlying metal by the contents of the tank. Such protective means are easily applied in the field without disturbing the position of the tank or its connections. Furthermore, the several shield parts employed are of such a nature that they are readily manufactured and supplied at a relatively low cost.

It will thus be seen that the invention accomplishes its objects and while it has been herein disclosed by reference to the details of preferred embodiments, it is to be understood that such disclosure is intended in an illustrative, rather than a limiting sense, as it is contemplated that various modifications in the construction and arrangement of the parts will readily occur to those skilled in the art, within the spirit of the invention and the scope of the appended claims.

I claim:

1. The combination with a processing container having an outwardly swaged nozzle and provided with a fused ceramic coating on the inner surfaces of said container and nozzle, of a repair shield comprising a plate of relatively thin, corrosion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle over said coating, means for securing said shield to said container, and means for sealing the space between said shield and the coated surfaces of said container and nozzle.

2. The combination with a processing container having an outwardly swaged nozzle and provided with a fused ceramic coating on the inner surfaces of said container and nozzle, of a repair shield comprising a plate of relatively thin, corrosion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle over said coating, means for securing said shield to said container, and a layer of corrosion-resisting cement between said shield and the coated surfaces of said container and nozzle, said plate and sleeve having marginal flanges turned toward said coated surfaces for retaining and protecting said cement.

3. The combination with a processing container having an outwardly swaged nozzle and provided with a fused ceramic coating on the inner surfaces of said container and nozzle, of a repair shield comprising a plate of relatively thin, corrosion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle over said coating, a plurality of bolts securing said plate to said container and means for sealing the space between said shield and the coated surfaces of said container and nozzle.

4. The combination with a processing container having an outwardly swaged nozzle and provided with a fused ceramic coating on the inner surfaces of said container and nozzle, of a repair shield comprising a plate of relatively thin, corrosion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle over said coating, a plurality of stud bolts securing said plate to said container and a layer of corrosion-resisting cement interposed between said shield and the coated surfaces of said container and nozzle, said plate and sleeve having marginal flanges turned toward said coated surfaces to retain and protect said cement.

5. The combination with a processing container having an outwardly swaged nozzle, a nozzle flange member welded to said nozzle and a fused ceramic coating on the inner surfaces of said container, nozzle and nozzle member, of a repair shield comprising a plate of relatively thin, corrosion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle and member over said coating and extending over the welded connection between said nozzle and member, means for securing said shield to said container, and means for sealing the space between said shield and the coated surfaces of said container, nozzle and nozzle member.

6. The combination with a processing container having an outwardly swaged nozzle, a nozzle flange member welded to said nozzle and a fused ceramic coating on the inner surfaces of said container, nozzle and member, of a repair shield comprising a plate of relatively thin, corrw sion-resisting sheet metal shaped to fit the coated inner surface of said container about said nozzle and having a sleeve spun outwardly therefrom to fit the throat of said nozzle and member over said coating and extending over the welded connection between said nozzle and member, stud bolts for securing said plate to said container, and a layer of corrosion-resisting cement for sealing the space between said shield and the coated surfaces of said container, nozzle and member, said plate and sleeve having marginalflanges turned toward said coated surfaces to retain and protect said cement.

References Cited in the file of this patent UNITED STATES PATENTS 360,993 Brown Apr. 12, 1887 373,703 Wagg Nov. 22, 1887 782,290 Tompkins Feb. 14, 1905 1,896,245 Nagel Feb. 7, 1933 1,948,391 Montgomery Feb. 20, 1934 2,239,509 Uecker Apr. 22, 1941 2,266,609 Martin Dec. 16, 1941 2,356,047 Geisinger Aug. 15, 1944 2,372,712 Crawford Apr. 3, 1945 2,374,733 Crawford May 1, 1945 2,374,763 Martin May 1 ,1945 2,381,890 Ebbets Aug. 14, 1945 2,445,273 Kennedy July 13, 1948 2,620,830 Schultz Dec. 9, 1952 

